¹H {one dimensional}

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Start            (BBO probe)

     Start up Topspin

     Change Samples

     Standard Shim Settings

     Lock

     Browse to group directory

     Create new filename for Both 13C & 1H

     Parameters

     Wobb

     Shim with BSMS keypad

Acquire 1H

     1H expno from 13C file

     ii rga zg efp

     Exand & Phase

     Check LineShape

     Set Parameters

            After 1H is Finished Acquiring -- Start 13C Acquisition

Processing 1H

            re 1 ................if you have started 13C in expno 2

     Calibrate

     Baseline Correction

     Integrals

     Peak Picking

Plotting

     Plot Editor

     Export Plots as .emf .pdf

     Stack Plots from display window

Finish

     Ready for next user

Advanced

     COSY    2D

     HomoNuclear-Decoupling    1D

     NOESY    2D

            Process NOESY with XwinNMR on SGI O2

            Process NOESY with TopSpin

     NOE Difference    1D

¹³ C {one dimensional}

Acquire Other Nuclei

     13C & DEPT-135

     31P

     19F ......................Requires the C/H/F probe to be in Magnet

     11B

     15N

     17O

     27Al

     33S

     35Cl

     39K

     59Co

     63Cu

     67Zn

     69Ga

     71Ga

     89Y

     111Cd

     113Cd

     119Sn

Finish

     Ready for next user

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XwinNMR  3.x   Instruction Manuals

Bruker Avance DRX-400 Instruction manuals

Setting up 1H and 13C ....................................31P & other X-nuclei {109Ag thru 31P}..................

XWINPLOT vers.3.1 ------1D plotting instructions....{Note: All future XwinNMR versions will only use XwinPlot for creating plots.}

Future Software ...--... TOPSPIN vers. 1.0 ...--... {To replace XwinNMR}

Advanced 1D plotting with XWINPLOT vers.3.1...................

Integration ..........................Signal-to-Noise...........................T1.........................Presaturation

Homo-Nuclear-Decoupling.............................Paramagnetics...................

Relaxation ...................... ...................... ...................... ...................... ......................

COSY Acquisition ...............................COSY Plottting (XWINPLOT)

HMQC / HMBC Acquisition ............................ QC/BC Plotting (XwinPlot)

Setting up TOCSY (presaturation)................

Setting up NOESY ..................

NOE Difference..................

Tuning C13 probe..................

Setting up Stack Plots..................

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Copyright © 2005, The University of Iowa, High Field NMR Central Research Facility, Office of the Vice President for Research

Last modified: Thursday     18-Nov-2005     J. Snyder

Contact information

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